Molecular Structure

Bruker Autoflex maX TOF-TOF MALDI Mass Spectrometer

Bruker Autoflex maX TOF/TOF MALDI Mass Spectrometer Mass Range : up to 500,000 Resolution : Linear Mode Positive Ion Mode            ≥ 1,100 @ m/z 12,361 (Cytochrome C) Negative Ion Mode          ≥ 2,500 @ m/z 1,569 (Glu-Fib) Reflector Mode Positive Ion Mode           >…

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Agilent Cary 60 UV-Vis Spectrophotometer

Agilent Cary 60 UV-Vis Spectrophotometer Optical Specifications Wavelength range190–1100 nm Xenon pulse lamp source Slit width1.5 nm Wavelength accuracy <±0.06 nm at 541.94 nm Wavelength reproducibility<±0.01 Photometric accuracy<±0.0007 Abs at 1 Abs (NIST 930e) Peltier cooled liquid sample holder Solid / Film sample holder Agilent Cary 60 UV-Vis Spectrophotometer Location: Hunter 247B Contact: Dr. Rakesh…

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Beckmann Coulter  DTX880  Photomultiplier Detector Multimode Plate Reader

Beckmann Coulter  DTX880  Photomultiplier Detector Multimode Plate Reader Fluorescence Intensity-Top Read Wavelength Range: Detection Limit (96-Well): Detection Limit(384-Well): Linear Dynamic Range: Read Time (Fly Mode):   Absorbance Wavelength Range: Indication Range: Accuracy: Reproducibility: Read Time: aaa 230-750 nm 1.5 fmol/100 µL fluorescein 1.5 fmol/100 µL fluorescein 5 decades 18 sec on 96-well; 37 sec on…

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Horiba iHR-320 Raman Spectrometer

Horiba iHR-320 Raman Spectrometer Aperture f/4.1 Spectral Range 150 to 1500 nm with 1200 g/mm grating 150 nm to 40 µm with appropriate gratings Grating Size 68 mm x 68 mm Number of Gratings on Turret 3 Flat Field Size 30 mm x 12 mm Resolution with Exit Slit and PMT 0.06 nm Wavelength Accuracy…

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Bruker Microflex MALDI-TOF Mass Spectrometer

Bruker Microflex MALDI-TOF Mass Spectrometer Mass Range : up to 300,000 Resolution : 15,000 Mass accuracy: 15 (int. calib.) [ppm] Laser: Nitrogen (337nm) Laser frequency [Hz]: 60 (MS) Bruker Microflex MALDI-TOF-MS Location: Hunter 240 Contact:  Dr. Rakesh Sachdeva

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Rigaku SmartLab Powder X-ray Diffractometer

Rigaku SmartLab Powder X-ray Diffractometer Cu sealed tube X-ray source. 10-position rotating sample changer. Theta-Theta goniometer. Zero background sample holders. HyPix-3000 2D HPAD detector. HT 1500 high temperature attachment for in-situ measurements. SmartLab Studio II software suite for instrument control, data processing, phase identification, Rietveld refinement. Access to the ICDD database. Location: Hunter 338 Contact:…

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Rigaku Ultima IV Powder X-ray Diffractometer

Rigaku Ultima IV Powder X-ray Diffractometer Cu sealed tube X-ray source. 10-position rotating sample changer. Theta-Theta goniometer. Zero background sample holders. Scintillation counter detector with monochromator. PDXL software suite for instrument control, data processing, phase identification. Access to the ICDD database. Location: Hunter 338 Contact: Dr. Colin McMillen

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Bruker D8 Quest Single Crystal X-ray diffractometer

Bruker D8 Quest Single Crystal X-ray diffractometer Mo sealed tube X-ray source. TRIUMPH monochromator. Fixed chi goniometer. Photon 100 CMOS detector. Oxford Cryostream 800 for data collections at 90-400 K. Apex 3 software suite for instrument control, data processing, structure refinement (SHELXTL). Access to the Cambridge Structural Database and the Inorganic Crystal Structure Database. Location:…

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Bruker D8 Venture Duo Single Crystal X-ray diffractometer

Bruker D8 Venture Duo Single Crystal X-ray diffractometer Mo and Cu microfocus X-ray sources. Kappa goniometer. Photon 2 CMOS detector. Oxford Cryostream 700 for data collections at 90-400 K. Apex 3 software suite for instrument control, data processing, structure refinement (SHELXTL). Access to the Cambridge Structural Database and the Inorganic Crystal Structure Database. Location: Hunter…

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Thermo Nicolet Nexus 670 FTIR Spectrometer

Spectral range: 7800–350 cm-1 optimized, mid-infrared KBr beamsplitter KBr optics: 4 cm-1 spectral resolution Signal-to-noise: Guaranteed: 5 seconds: 8000:1 (peak to peak), 1 minute: 22,000:1 (peak to peak), Typical: 1 minute: 28,000:1 (peak to peak) Spectral resolution: better than 0.8 cm-1; better than 0.5 cm-1 using aperture Wavelength precision: 0.01 cm-1 at 2000 cm-1 Detector:…

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Nicolet iS5 FTIR Spectrometer

Spectral range: 7800–350 cm-1 optimized, mid-infrared KBr beamsplitter Signal-to noise: guaranteed: 5 seconds: 8000:1 (peak to peak), typical: 1 minute: 28,000:1 (peak to peak) Spectral resolution: better than 0.8 cm-1; better than 0.5 cm-1 using aperture Wavelength precision:0.01 cm-1 at 2000 cm-1 KBr optics: 4 cm-1 spectral resolution Detector: fast recovery deuterated triglycine sulfate (DTGS)…

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Shimadzu IRAffinity-1S FTIR Spectrometer

Accessory : MIRacle 10 ATR, transmission Beam splitter : Germanium-coated KBr Light source : High-energy ceramic light source Detector : DLATGS detector equipped with temperature control mechanism Wavenumber range: 7,800 to 350 cm-1 Resolution : 0.5, 1, 2, 4, 8, 16 cm-1 Shimadzu IRAffinity-IS Location: Hunter 247B Contact: Dr. Rakesh Sachdeva

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Bruker Avance Neo500 Nuclear Magnetic Resonance Spectrometer

High Resolution Multinuclear two channel NMR spectrometer. This  spectrometer is equipped with a 5 mm Prodigy CryoProbe with Auto Tune and Match (ATM) capability over its full range of 1H, 19F and X-Broadband (31P-15N) nuclei. The Prodigy delivers tremendous boosts in sensitivity (by factor of 2 to 3) over room temperature probes. Software used:   Topspin…

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Bruker Avance-300 Nuclear Magnetic Resonance Spectrometer

High Resolution Multinuclear NMR spectrometer. Ideal instrument for fast routine NMR spectra of organic compounds. Installed Quadro Nucleus Probe allows the measurement of four different nuclei: 1H, 19F, 13C and 31P. The QNP Control Module allows instant automatic switching between the nuclei. VT temperature control includes a cooling unit with low temperature capability up to…

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Bruker Avance 500 Nuclear Magnetic Resonance Spectrometer

High Resolution Multinuclear NMR spectrometer equipped with  5 mm Broadband Observe (BBO) Probe with Auto Tune and Match (ATM) capability over its full range of 1H and X-Broadband (31P-15N) nuclei and typically runs high resolution NMR spectra in liquids. It is also capable of running CP-MAS experiments in solid state. 4-mm CP-MAS probe is available…

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Shimadzu QP2010 Plus with AOC 20i+s autosampler

Shimadzu QP2010 Plus with AOC 20i+s autosampler Injector: Split / Splitless Detector: MS, FID Column: SH-Rxi-Sil5MS, 30m x 0.25mm x 0.25 μm SH-Rxi-5MS, 15m x 0.25mm x 0.25 μm Mass range: m/z to 1,000 El scan S/N: 1pg octa fluoronapthalene m/z 272 S/N ≥ 600 (helium gas) High-speed scan rate: 10,000 u/sec Shimadzu QP2010 GCMS…

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Jeol ECX 300 Nuclear Magnetic Resonance Spectrometer

High Resolution Multinuclear NMR spectrometer. Ideal instrument for fast routine NMR spectra of organic compounds. With the JEOL AutoTune 5mm NMR Probe all multi-nuclear spectra from 1H, 19F, 31P to 15N are available under computer control. Software used:   Delta 4.3.6 NMR Frequency:  300 MHz Location   AMRL Jeol ECX300 NMR Location: AMRL Contact: Dr. Alex Kitaygorodskiy

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Agilent 6545 QTOF LC-MS/MS Mass Spectrometer

Agilent 6545 QTOF LC-MS/MS Mass Spectrometer Mass range – 50-10,000 m/z Dynamic range : 5 orders of magnitude Resolving power : 45,000 FWHM at m/z 2722 RMS :   0.8 ppm at (M+H)+ ion m/z 609.2807 (reserpine) in MS mode better than 2 ppm RMS on m/z 397 of reserpine in MS/MS mode. Spectral acquisition…

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Nicolet Magna IR 550 FTIR Spectrometer

Measuring range: 350 – 7400 cm-1 Spectral resolution: 0.5 cm-1 Beamsplitters: KBr (350 – 7400 cm-1) Suited for experiments in step scan, linear scan, time resolved, and rapid scan spectroscopy TM Interferometer Rapid scanning interferometer. Continuous dynamic alignment of interferometer. 2 mirrors from beamsplitter to detector: single parabolic mirror from beamsplitter to sample: single ellipsoidal mirror…

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Agilent 8453 UV-Vis Spectrophotometer

Optical Specifications Wavelength range190–1100 nm Slit width1 nm Wavelength accuracy <±0.5 nm(NIST 2034) Wavelength reproducibility<±0.02 nm ten consecutive scans (NIST 2034) Photometric accuracy<±0.005 A at 1 A (NIST 930e) Agilent 8453 UV-Vis Spectrophotometer Location: Hunter 319 Contact: Dr. Rakesh Sachdeva

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