{"id":14028,"date":"2025-04-25T01:52:18","date_gmt":"2025-04-25T01:52:18","guid":{"rendered":"https:\/\/scienceweb.clemson.edu\/uacl-new\/?p=14028"},"modified":"2025-11-06T02:08:19","modified_gmt":"2025-11-06T02:08:19","slug":"reu-project-03","status":"publish","type":"post","link":"https:\/\/scienceweb.clemson.edu\/uacl\/reu-project-03\/","title":{"rendered":"Stability of H-Bonding in Aqueous Mixtures of NADES"},"content":{"rendered":"\t\t<div data-elementor-type=\"wp-post\" data-elementor-id=\"14028\" class=\"elementor elementor-14028\" data-elementor-post-type=\"post\">\n\t\t\t\t<div class=\"elementor-element elementor-element-ea7d30e e-flex e-con-boxed mk-enable-fade-animation-none mk-sticky-column-false mk-sticky-column-disable-tablet e-con e-parent\" data-id=\"ea7d30e\" data-element_type=\"container\" data-e-type=\"container\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_sticky&quot;:&quot;false&quot;}\">\n\t\t\t\t\t<div class=\"e-con-inner\">\n\t\t<div class=\"elementor-element elementor-element-8a52b07 e-con-full e-flex mk-enable-fade-animation-none mk-sticky-column-false mk-sticky-column-disable-tablet e-con e-child\" data-id=\"8a52b07\" data-element_type=\"container\" data-e-type=\"container\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_sticky&quot;:&quot;false&quot;}\">\n\t\t\t\t<div class=\"elementor-element elementor-element-2ee2ebd mk-enable-fade-animation-none elementor-widget elementor-widget-theme-post-featured-image elementor-widget-image\" data-id=\"2ee2ebd\" data-element_type=\"widget\" data-e-type=\"widget\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_infinite&quot;:&quot;false&quot;,&quot;mk_ext_is_scrollme&quot;:&quot;false&quot;}\" data-widget_type=\"theme-post-featured-image.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t\t\t\t\t\t\t<img fetchpriority=\"high\" decoding=\"async\" width=\"750\" height=\"772\" src=\"https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/REU_project_03.png\" class=\"attachment-large size-large wp-image-14102\" alt=\"REU project 03\" srcset=\"https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/REU_project_03.png 750w, https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/REU_project_03-291x300.png 291w\" sizes=\"(max-width: 750px) 100vw, 750px\" \/>\t\t\t\t\t\t\t\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t<div class=\"elementor-element elementor-element-58afc33 e-con-full e-flex mk-enable-fade-animation-none mk-sticky-column-false mk-sticky-column-disable-tablet e-con e-child\" data-id=\"58afc33\" data-element_type=\"container\" data-e-type=\"container\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_sticky&quot;:&quot;false&quot;}\">\n\t\t\t\t<div class=\"elementor-element elementor-element-5212c875 mk-enable-fade-animation-none elementor-widget elementor-widget-text-editor\" data-id=\"5212c875\" data-element_type=\"widget\" data-e-type=\"widget\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_infinite&quot;:&quot;false&quot;,&quot;mk_ext_is_scrollme&quot;:&quot;false&quot;}\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t<p><span style=\"color: #000000\">Most reported NADES are highly viscous at room temperature, a characteristic that is attributed to the formation of the hydrogen bonding network among their components and that represents the most pressing obstacle for their implementation in a wide variety of fields. Although different strategies have been presented to overcome this issue, adding water is probably the most effective one . In this regard, some authors state that the addition of water does not affect the interaction of the main components in a NADES, while others argue that water has the potential to modulate the microstructure of DES and the resulting properties, potentially affecting the number of hydrogen bonds as well as the strength of the interaction. Moreover, excessive additions (&gt;40% mole ratio) could compete with the hydrogen bond network\u00a0and destabilize these eutectic mixtures.\u00a0Aiming to gain a detailed understanding of the role of hydrogen bonding in these solvents, participants involved with this project will use nuclear Overhauser effect (NOE) experiments in the gel phase to determine both the <sup>1<\/sup>H-<sup>1<\/sup>H distances between DES components and the average rotational correlation times of the constituent molecules. Measurements will be made on samples containing differing amounts of water to determine how much water is required to disrupt the hydrogen-bond interactions responsible for DES formation. The high-resolution spectral information this probe provides will also enable participants to observe changes in chemical shifts upon NADES formation. To gain a molecular understanding of the chemical interactions behind the formation and de-stabilization of DES, the experimental aspects of this project will be complemented by computational approaches. For example, participants will have the opportunity to use DFT geometry optimizations to confirm the presence of hydrogen bonds. As overall goals, this project will provide participants the opportunity to work full-time in NMR spectroscopy, generate basic knowledge to enable expanding the use of DES as solvents, and enable determining which systems will be compatible with water and which ones will not.<\/span><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t<div class=\"elementor-element elementor-element-4de53ad e-flex e-con-boxed mk-enable-fade-animation-none mk-sticky-column-false mk-sticky-column-disable-tablet e-con e-parent\" data-id=\"4de53ad\" data-element_type=\"container\" data-e-type=\"container\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_sticky&quot;:&quot;false&quot;}\">\n\t\t\t\t\t<div class=\"e-con-inner\">\n\t\t\t\t<div class=\"elementor-element elementor-element-b939151 mk-enable-fade-animation-none elementor-widget elementor-widget-spacer\" data-id=\"b939151\" data-element_type=\"widget\" data-e-type=\"widget\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_infinite&quot;:&quot;false&quot;,&quot;mk_ext_is_scrollme&quot;:&quot;false&quot;}\" data-widget_type=\"spacer.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t<div class=\"elementor-spacer\">\n\t\t\t<div class=\"elementor-spacer-inner\"><\/div>\n\t\t<\/div>\n\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t<div class=\"elementor-element elementor-element-3ea0e74 e-flex e-con-boxed mk-enable-fade-animation-none mk-sticky-column-false mk-sticky-column-disable-tablet e-con e-parent\" data-id=\"3ea0e74\" data-element_type=\"container\" data-e-type=\"container\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_sticky&quot;:&quot;false&quot;}\">\n\t\t\t\t\t<div class=\"e-con-inner\">\n\t\t<div class=\"elementor-element elementor-element-0da052f e-con-full e-flex mk-enable-fade-animation-none mk-sticky-column-false mk-sticky-column-disable-tablet e-con e-child\" data-id=\"0da052f\" data-element_type=\"container\" data-e-type=\"container\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_sticky&quot;:&quot;false&quot;}\">\n\t\t\t\t<div class=\"elementor-element elementor-element-1b5e2a5 mk-enable-fade-animation-none elementor-widget elementor-widget-image\" data-id=\"1b5e2a5\" data-element_type=\"widget\" data-e-type=\"widget\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_infinite&quot;:&quot;false&quot;,&quot;mk_ext_is_scrollme&quot;:&quot;false&quot;}\" data-widget_type=\"image.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t\t\t\t\t\t\t<img decoding=\"async\" width=\"282\" height=\"424\" data-src=\"https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/Leah_Casabianca.jpg\" class=\"attachment-large size-large wp-image-14731 lazyload\" alt=\"Leah Casabianca\" data-srcset=\"https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/Leah_Casabianca.jpg 282w, https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/Leah_Casabianca-200x300.jpg 200w\" data-sizes=\"(max-width: 282px) 100vw, 282px\" src=\"data:image\/svg+xml;base64,PHN2ZyB3aWR0aD0iMSIgaGVpZ2h0PSIxIiB4bWxucz0iaHR0cDovL3d3dy53My5vcmcvMjAwMC9zdmciPjwvc3ZnPg==\" style=\"--smush-placeholder-width: 282px; --smush-placeholder-aspect-ratio: 282\/424;\" \/>\t\t\t\t\t\t\t\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t<div class=\"elementor-element elementor-element-5759a88 e-con-full e-flex mk-enable-fade-animation-none mk-sticky-column-false mk-sticky-column-disable-tablet e-con e-child\" data-id=\"5759a88\" data-element_type=\"container\" data-e-type=\"container\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_sticky&quot;:&quot;false&quot;}\">\n\t\t\t\t<div class=\"elementor-element elementor-element-87f4bd9 mk-enable-fade-animation-none elementor-widget elementor-widget-text-editor\" data-id=\"87f4bd9\" data-element_type=\"widget\" data-e-type=\"widget\" data-settings=\"{&quot;mk-animation-effect&quot;:&quot;none&quot;,&quot;mk_ext_is_infinite&quot;:&quot;false&quot;,&quot;mk_ext_is_scrollme&quot;:&quot;false&quot;}\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t\t\t<p><span style=\"color: #000000\"><strong>Students working in this project will be mentored by Dr. Leah Casabianca, at Clemson University<\/strong><\/span><\/p><p><a href=\"https:\/\/www.clemson.edu\/science\/academics\/departments\/chemistry\/about\/profiles\/lcasabi\"><img decoding=\"async\" class=\"size-full wp-image-14115 lazyload\" title=\"icons8 website\" data-src=\"https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/icons8-website.gif\" alt=\"icons8 website\" width=\"50\" height=\"50\" src=\"data:image\/svg+xml;base64,PHN2ZyB3aWR0aD0iMSIgaGVpZ2h0PSIxIiB4bWxucz0iaHR0cDovL3d3dy53My5vcmcvMjAwMC9zdmciPjwvc3ZnPg==\" style=\"--smush-placeholder-width: 50px; --smush-placeholder-aspect-ratio: 50\/50;\" \/><\/a> <a href=\"https:\/\/scholar.google.com\/citations?user=N3uALTEAAAAJ&amp;hl=en\"><img decoding=\"async\" class=\"size-full wp-image-14116 lazyload\" title=\"icons8 google scholar 50\" data-src=\"https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/icons8-google-scholar-50.png\" alt=\"icons8 google scholar 50\" width=\"50\" height=\"50\" data-srcset=\"https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/icons8-google-scholar-50.png 50w, https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/elementor\/thumbs\/icons8-google-scholar-50-r53orhp59nh1i1yl0nelevkoz1i2lwo3xev7el2dy6.png 35w\" data-sizes=\"(max-width: 50px) 100vw, 50px\" src=\"data:image\/svg+xml;base64,PHN2ZyB3aWR0aD0iMSIgaGVpZ2h0PSIxIiB4bWxucz0iaHR0cDovL3d3dy53My5vcmcvMjAwMC9zdmciPjwvc3ZnPg==\" style=\"--smush-placeholder-width: 50px; --smush-placeholder-aspect-ratio: 50\/50;\" \/><\/a><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t","protected":false},"excerpt":{"rendered":"<p>Most reported NADES are highly viscous at room temperature, a characteristic that is attributed to the formation of the hydrogen bonding network among their components and that represents the most pressing obstacle for their implementation in a wide variety of fields. Although different strategies have been presented to overcome this issue, adding water is probably the most effective one . In this regard, some authors state that the addition of water does not affect the interaction of the main components in a NADES, while others argue that water has the potential to modulate the microstructure of DES and the resulting [&hellip;]<\/p>\n","protected":false},"author":20,"featured_media":14102,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":"","_links_to":"","_links_to_target":""},"categories":[158],"tags":[],"class_list":["post-14028","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-reu_03_projects"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v28.4 - https:\/\/yoast.com\/product\/yoast-seo-wordpress\/ -->\n<title>Stability of H-Bonding in Aqueous Mixtures of NADES - Microanalytical Chemistry Lab<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/scienceweb.clemson.edu\/uacl\/reu-project-03\/\" \/>\n<meta property=\"og:locale\" content=\"en_US\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Stability of H-Bonding in Aqueous Mixtures of NADES - Microanalytical Chemistry Lab\" \/>\n<meta property=\"og:description\" content=\"Most reported NADES are highly viscous at room temperature, a characteristic that is attributed to the formation of the hydrogen bonding network among their components and that represents the most pressing obstacle for their implementation in a wide variety of fields. Although different strategies have been presented to overcome this issue, adding water is probably the most effective one . In this regard, some authors state that the addition of water does not affect the interaction of the main components in a NADES, while others argue that water has the potential to modulate the microstructure of DES and the resulting [&hellip;]\" \/>\n<meta property=\"og:url\" content=\"https:\/\/scienceweb.clemson.edu\/uacl\/reu-project-03\/\" \/>\n<meta property=\"og:site_name\" content=\"Microanalytical Chemistry Lab\" \/>\n<meta property=\"article:published_time\" content=\"2025-04-25T01:52:18+00:00\" \/>\n<meta property=\"article:modified_time\" content=\"2025-11-06T02:08:19+00:00\" \/>\n<meta property=\"og:image\" content=\"https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/REU_project_03.png\" \/>\n\t<meta property=\"og:image:width\" content=\"750\" \/>\n\t<meta property=\"og:image:height\" content=\"772\" \/>\n\t<meta property=\"og:image:type\" content=\"image\/png\" \/>\n<meta name=\"author\" content=\"CDG\" \/>\n<meta name=\"twitter:card\" content=\"summary_large_image\" \/>\n<meta name=\"twitter:creator\" content=\"@MicroAnalytic11\" \/>\n<meta name=\"twitter:label1\" content=\"Written by\" \/>\n\t<meta name=\"twitter:data1\" content=\"CDG\" \/>\n\t<meta name=\"twitter:label2\" content=\"Est. reading time\" \/>\n\t<meta name=\"twitter:data2\" content=\"3 minutes\" \/>\n<script type=\"application\/ld+json\" class=\"yoast-schema-graph\">{\"@context\":\"https:\\\/\\\/schema.org\",\"@graph\":[{\"@type\":\"Article\",\"@id\":\"https:\\\/\\\/scienceweb.clemson.edu\\\/uacl\\\/reu-project-03\\\/#article\",\"isPartOf\":{\"@id\":\"https:\\\/\\\/scienceweb.clemson.edu\\\/uacl\\\/reu-project-03\\\/\"},\"author\":{\"name\":\"CDG\",\"@id\":\"https:\\\/\\\/scienceweb.clemson.edu\\\/uacl\\\/#\\\/schema\\\/person\\\/84db2eae9183261b17b2280646687289\"},\"headline\":\"Stability of H-Bonding in Aqueous Mixtures of NADES\",\"datePublished\":\"2025-04-25T01:52:18+00:00\",\"dateModified\":\"2025-11-06T02:08:19+00:00\",\"mainEntityOfPage\":{\"@id\":\"https:\\\/\\\/scienceweb.clemson.edu\\\/uacl\\\/reu-project-03\\\/\"},\"wordCount\":344,\"publisher\":{\"@id\":\"https:\\\/\\\/scienceweb.clemson.edu\\\/uacl\\\/#organization\"},\"image\":{\"@id\":\"https:\\\/\\\/scienceweb.clemson.edu\\\/uacl\\\/reu-project-03\\\/#primaryimage\"},\"thumbnailUrl\":\"https:\\\/\\\/scienceweb.clemson.edu\\\/uacl\\\/wp-content\\\/uploads\\\/sites\\\/46\\\/2025\\\/04\\\/REU_project_03.png\",\"articleSection\":[\"REU_03_projects\"],\"inLanguage\":\"en-US\"},{\"@type\":\"WebPage\",\"@id\":\"https:\\\/\\\/scienceweb.clemson.edu\\\/uacl\\\/reu-project-03\\\/\",\"url\":\"https:\\\/\\\/scienceweb.clemson.edu\\\/uacl\\\/reu-project-03\\\/\",\"name\":\"Stability of H-Bonding in Aqueous Mixtures of NADES - 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Although different strategies have been presented to overcome this issue, adding water is probably the most effective one . In this regard, some authors state that the addition of water does not affect the interaction of the main components in a NADES, while others argue that water has the potential to modulate the microstructure of DES and the resulting [&hellip;]","og_url":"https:\/\/scienceweb.clemson.edu\/uacl\/reu-project-03\/","og_site_name":"Microanalytical Chemistry Lab","article_published_time":"2025-04-25T01:52:18+00:00","article_modified_time":"2025-11-06T02:08:19+00:00","og_image":[{"width":750,"height":772,"url":"https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/REU_project_03.png","type":"image\/png"}],"author":"CDG","twitter_card":"summary_large_image","twitter_creator":"@MicroAnalytic11","twitter_misc":{"Written by":"CDG","Est. reading time":"3 minutes"},"schema":{"@context":"https:\/\/schema.org","@graph":[{"@type":"Article","@id":"https:\/\/scienceweb.clemson.edu\/uacl\/reu-project-03\/#article","isPartOf":{"@id":"https:\/\/scienceweb.clemson.edu\/uacl\/reu-project-03\/"},"author":{"name":"CDG","@id":"https:\/\/scienceweb.clemson.edu\/uacl\/#\/schema\/person\/84db2eae9183261b17b2280646687289"},"headline":"Stability of H-Bonding in Aqueous Mixtures of NADES","datePublished":"2025-04-25T01:52:18+00:00","dateModified":"2025-11-06T02:08:19+00:00","mainEntityOfPage":{"@id":"https:\/\/scienceweb.clemson.edu\/uacl\/reu-project-03\/"},"wordCount":344,"publisher":{"@id":"https:\/\/scienceweb.clemson.edu\/uacl\/#organization"},"image":{"@id":"https:\/\/scienceweb.clemson.edu\/uacl\/reu-project-03\/#primaryimage"},"thumbnailUrl":"https:\/\/scienceweb.clemson.edu\/uacl\/wp-content\/uploads\/sites\/46\/2025\/04\/REU_project_03.png","articleSection":["REU_03_projects"],"inLanguage":"en-US"},{"@type":"WebPage","@id":"https:\/\/scienceweb.clemson.edu\/uacl\/reu-project-03\/","url":"https:\/\/scienceweb.clemson.edu\/uacl\/reu-project-03\/","name":"Stability of H-Bonding in Aqueous Mixtures of NADES - 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